1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

Base Information

Chemical Name:1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane
CAS No.:107519-64-2
Molecular Formula:C₁₆H₁₁Cl₃N₄O₁₀
Molecular Weight:525.643
Hs Code.:

Synonyms:1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

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Chemical Property of 1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

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Technology Process of 1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

There total 3 articles about 1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30667-99-3
1,1,1-trichloro-2-(2-methoxyphenyl)-2-(4-methoxyphenyl)ethane

: 107519-64-2
1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

Guidance literature:: With nitric acid; at 0 ℃;
DOI:10.1021/ja01176a087

Reference yield:

: 58369-59-8
2-methoxy-α-(trichloromethyl)benzyl alcohol

: 107519-64-2
1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: concentrated sulfuric acid; glacial acetic acid / 0 °C

2: fuming nitric acid / 0 °C

With sulfuric acid; nitric acid; acetic acid;
DOI:10.1021/ja01176a087

Reference yield:

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 107519-64-2
1,1,1-trichloro-2-(2-methoxy-3,5-dinitro-phenyl)-2-(4-methoxy-3,5-dinitro-phenyl)-ethane

Guidance literature:: Multi-step reaction with 3 steps

2: concentrated sulfuric acid; glacial acetic acid / 0 °C

3: fuming nitric acid / 0 °C

With sulfuric acid; nitric acid; acetic acid;
DOI:10.1021/ja01176a087