[3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane

Base Information

• Chemical Name: [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane
• CAS No.: 163396-63-2
• Molecular Formula: C₂₄H₄₂O₄Si
• Molecular Weight: 422.681

Synonyms:[3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane

Chemical Property of [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane

Chemical Property:

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Technology Process of [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane

There total 3 articles about [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

[3-(1-tert-Butoxy-2-isopropyl-3-methyl-but-1-enyl)-phenoxy]-tert-butyl-dimethyl-silane (163396-59-6) → [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane (163396-63-2)

Guidance literature:

With oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at -78 ℃; for 2h; Irradiation;

DOI:10.1016/S0040-4020(99)00124-6

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane (163396-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaSEt, 2.) K₂CO₃ / 1.) DMF, reflux, 3 h, 2.) DMF, room temperature

2: 69 percent / oxygen, tetraphenylporphin / CH₂Cl₂ / 2 h / -78 °C / Irradiation

With oxygen; 5,15,10,20-tetraphenylporphyrin; potassium carbonate; sodium thioethylate; In dichloromethane;

DOI:10.1016/S0040-4020(99)00124-6

Reference yield:

1-(1-tert-Butoxy-2-isopropyl-3-methyl-but-1-enyl)-3-methoxy-benzene (163396-55-2) → [3-(3-tert-Butoxy-4,4-diisopropyl-[1,2]dioxetan-3-yl)-phenoxy]-tert-butyl-dimethyl-silane (163396-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaSEt, 2.) K₂CO₃ / 1.) DMF, reflux, 3 h, 2.) DMF, room temperature

2: 69 percent / oxygen, tetraphenylporphin / CH₂Cl₂ / 2 h / -78 °C / Irradiation

With oxygen; 5,15,10,20-tetraphenylporphyrin; potassium carbonate; sodium thioethylate; In dichloromethane;

DOI:10.1016/S0040-4020(99)00124-6

upstream raw materials:

[3-(1-tert-Butoxy-2-isopropyl-3-methyl-but-1-enyl)-phenoxy]-tert-butyl-dimethyl-silane

tert-butyldimethylsilyl chloride

1-(1-tert-Butoxy-2-isopropyl-3-methyl-but-1-enyl)-3-methoxy-benzene

Downstream raw materials:

2,4-dimethylpentan-3-one

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