Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

Base Information

Chemical Name:Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside
CAS No.:81312-33-6
Molecular Formula:C₁₆H₁₇F₃N₂O₇
Molecular Weight:406.315
Hs Code.:

Synonyms:Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

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Chemical Property of Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

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Technology Process of Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

There total 1 articles about Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 56390-10-4
methyl 2,3,6-trideoxy-3-(trifluoroacetamido)-α-L-lyxo-hexopyranoside

: 122-04-3
4-nitro-benzoyl chloride

: 81312-33-6
Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

Guidance literature:: In pyridine; water; at 0 ℃; for 17h;
DOI:10.1016/S0008-6215(00)80669-2

Reference yield: 65.0%

: 81312-33-6
Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 81312-34-7
2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose

: 81312-35-8
2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-lyxo-hexopyranose

Guidance literature:: With trifluoroacetic acid; at 25 ℃;
DOI:10.1016/S0008-6215(00)80669-2

Reference yield:

: 81312-33-6
Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 81312-37-0
ethyl 2-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-lyxo-hexopyranosyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 80percent trifluoroacetic acid / 25 °C

2: 15.4 percent / dimethylformamide / 48 h / Heating

With trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80669-2