2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose

Base Information

• Chemical Name: 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose
• CAS No.: 81312-34-7
• Molecular Formula: C₁₅H₁₅F₃N₂O₇
• Molecular Weight: 392.289

Synonyms:2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose

Chemical Property of 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose

Chemical Property:

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Technology Process of 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose

There total 17 articles about 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

methyl-2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-xylo-hexopyranoside (76753-24-7) → 2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α,β-L-xylo-hexopyranose (76753-25-8,76753-31-6,76753-32-7,76760-23-1,81312-34-7,81312-35-8)

Guidance literature:

With acetic acid; In water; for 1.25h; Heating;

DOI:10.1016/S0008-6215(00)84673-X

Reference yield: 65.0%

Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside (81312-33-6) → 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranose (81312-34-7) + 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-lyxo-hexopyranose (81312-35-8)

Guidance literature:

With trifluoroacetic acid; at 25 ℃;

DOI:10.1016/S0008-6215(00)80669-2

Reference yield:

methyl-2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-D-arabino-hexopyranoside (76753-26-9) → 2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-D-arabino-hexopyranose (76753-25-8,76753-31-6,76753-32-7,76760-23-1,81312-34-7,81312-35-8)

Guidance literature:

With acetic acid; In water; for 48h; Yield given; Heating;

DOI:10.1016/S0008-6215(00)84673-X

upstream raw materials:

Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

methyl-2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-xylo-hexopyranoside

methyl-3-amino-2,3,6-tridesoxy-β-L-xylo-hexopyranoside

methyl-2,3,6-tridesoxy-3-trifluoroacetamido-β-L-xylo-hexopyranoside

Downstream raw materials:

4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1S,3R)-3-acetyl-5,8-dimethoxy-isochroman-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1R,3S)-3-acetyl-5,8-dimethoxy-isochroman-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

1-O-tert-butyldimethylsilyl 4-O-p-nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetamido-β-L-lyxo-hexopyranoside

4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1S,3R)-3-acetyl-6-hydroxy-5,12-dioxo-3,4,5,12-tetrahydro-1H-2-oxa-naphthacen-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

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