2-azidobenzenesulfonic acid

Base Information

Chemical Name:2-azidobenzenesulfonic acid
CAS No.:71236-07-2
Molecular Formula:C₆H₅N₃O₃S
Molecular Weight:199.19
Hs Code.:

Synonyms:2-azidobenzenesulfonic acid

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Chemical Property of 2-azidobenzenesulfonic acid

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Technology Process of 2-azidobenzenesulfonic acid

There total 1 articles about 2-azidobenzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 88-21-1
2-amino-1-benzenesulfonic acid

: 71236-07-2
2-azidobenzenesulfonic acid

Guidance literature:: 2-amino-1-benzenesulfonic acid; With sulfuric acid; sodium nitrite; In water; at 0 ℃; for 0.5h; Inert atmosphere;

With sodium azide; In water; at 0 - 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c03838

Reference yield: 96.0%

: 71236-07-2
2-azidobenzenesulfonic acid

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 1248341-66-3
(S)-(1-(2'-azidobenzenesulfonyl)pyrrolidin-2-yl)methanol

Guidance literature:: 2-azidobenzenesulfonic acid; With oxalyl dichloride; In dichloromethane;

(S)-1-Pyrrolidin-2-yl-methanol; With potassium carbonate; In dichloromethane; water; at 20 ℃;
DOI:10.1016/j.tetlet.2010.07.050

Reference yield: 90.0%

: 71236-07-2
2-azidobenzenesulfonic acid

: 14415-44-2
6-aminocoumarin

: 1394932-06-9
2-azido-N-(2-oxo-2H-chromen-6-yl)benzenesulfonamide

Guidance literature:: 2-azidobenzenesulfonic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 3h; Reflux;

6-aminocoumarin; With sodium acetate; In methanol; water; at 60 ℃; for 1h;
DOI:10.1016/j.tet.2012.07.040