Monomethyl 3-Hydroxypentanedioic Acid

Base Information

Chemical Name:Monomethyl 3-Hydroxypentanedioic Acid
CAS No.:109462-19-3
Molecular Formula:C₆H₁₀O₅
Molecular Weight:162.142
Hs Code.:

Synonyms:Monomethyl 3-Hydroxypentanedioic Acid

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Chemical Property of Monomethyl 3-Hydroxypentanedioic Acid

Chemical Property:

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Technology Process of Monomethyl 3-Hydroxypentanedioic Acid

There total 1 articles about Monomethyl 3-Hydroxypentanedioic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 542-05-2
acetonedicarboxylic acid

: 638-18-6
diethyl 3-hydroxypentanedioate

: 109462-19-3
Monomethyl 3-Hydroxypentanedioic Acid

Guidance literature:: With potassium hydroxide; sodium tetrahydroborate; for 0.333333h;
DOI:10.1021/es0620181

Reference yield:

: 109462-19-3
Monomethyl 3-Hydroxypentanedioic Acid

: methyl 5-bromo-3-<<(S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionyl>oxy>pentanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 19.4 g / imidazole / dimethylformamide / 12 h / Ambient temperature

2: 84 percent / K₂CO₃ / methanol; tetrahydrofuran; H₂O / 1 h / Ambient temperature

3: 76 percent / BH₃*Me₂S / tetrahydrofuran / 1.5 h

4: 71 percent / Ph₃P, CBr₄, pyridine / diethyl ether / 2 h / Ambient temperature

5: aq. HCl / tetrahydrofuran

6: pyridine / CH₂Cl₂

With pyridine; 1H-imidazole; hydrogenchloride; carbon tetrabromide; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19870700118

Reference yield:

: 109462-19-3
Monomethyl 3-Hydroxypentanedioic Acid

: p-nitrobenzyl methyl 3-(camphanoyloxy)glutarate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.7 g / H₂O; ethanol / 1 h / Heating; pH = 6.0

2: 94 percent / pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; In ethanol; dichloromethane; water;
DOI:10.1002/hlca.19870700118