1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol

Base Information

• Chemical Name: 1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol
• CAS No.: 1346261-55-9
• Molecular Formula: C₁₈H₂₆BClO₃
• Molecular Weight: 336.667

Synonyms:1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol

Chemical Property of 1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol

Chemical Property:

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Technology Process of 1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol

There total 1 articles about 1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H39B2ClO2 + isobutyraldehyde (78-84-2) → 1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol (1346261-55-9)

Guidance literature:

C₂₆H₃₉B₂ClO₂; With dimethyl zinc(II); In toluene; at -78 ℃; for 0.5h; Inert atmosphere;

isobutyraldehyde; In toluene; at -10 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol202588g

Reference yield: 75.0%

1-(4-chlorophenyl)-4-methyl-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pent-1-en-3-ol (1346261-55-9) + N-aminophthalamide (1875-48-5) → 2-(3-(4-chlorophenyl)-2-(1-hydroxy-2-methylpropyl)-2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)aziridin-1-yl)isoindoline-1,3-dione

Guidance literature:

With [bis(acetoxy)iodo]benzene; potassium carbonate; In dichloromethane; at 0 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/ol202588g

upstream raw materials:

isobutyraldehyde

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