C₂₆H₄₂O₅Si

Base Information

Chemical Name:C₂₆H₄₂O₅Si
CAS No.:1252660-28-8
Molecular Formula:C₂₆H₄₂O₅Si
Molecular Weight:462.702
Hs Code.:

C<sub>26</sub>H<sub>42</sub>O<sub>5</sub>Si

Synonyms:C₂₆H₄₂O₅Si

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Chemical Property of C₂₆H₄₂O₅Si

Chemical Property:

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Technology Process of C₂₆H₄₂O₅Si

There total 7 articles about C₂₆H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1252660-27-7
C₂₃H₃₆O₄Si

: 15448-47-2
(R)-propylene oxide

: 1252660-28-8
C₂₆H₄₂O₅Si

Guidance literature:: C₂₃H₃₆O₄Si; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; at -78 ℃; for 0.1h; Inert atmosphere;

(R)-propylene oxide; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol102201z

Reference yield:

: 60856-63-5
(2R)-(-)-3,3-dimethylbutane-1,2,4-triol

: 1252660-28-8
C₂₆H₄₂O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / Inert atmosphere

3: tetrahydrofuran / Inert atmosphere

4: potassium hydride; Trimethylenediamine / 0 °C / Inert atmosphere

5: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

6: n-butyllithium; boron trifluoride diethyl etherate / Inert atmosphere

With 1H-imidazole; n-butyllithium; oxalyl dichloride; boron trifluoride diethyl etherate; potassium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; Trimethylenediamine; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: Swern oxidation;
DOI:10.3762/bjoc.7.66

Reference yield:

: 599-04-2
(R)-Pantolacton

: 1252660-28-8
C₂₆H₄₂O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

2: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere

3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / Inert atmosphere

4: tetrahydrofuran / Inert atmosphere

5: potassium hydride; Trimethylenediamine / 0 °C / Inert atmosphere

6: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

7: n-butyllithium; boron trifluoride diethyl etherate / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; boron trifluoride diethyl etherate; potassium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; Trimethylenediamine; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 3: Swern oxidation;
DOI:10.3762/bjoc.7.66