epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

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Chemical Name:epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine
CAS No.:1432025-45-0
Molecular Formula:C₂₆H₃₃N₁₅O₁₀
Molecular Weight:715.643
Hs Code.:

Synonyms:epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

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Chemical Property of epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

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Technology Process of epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

There total 4 articles about epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5006-66-6
6-hydroxy-3-pyridinecarboxylic acid

: 1432025-39-2
epi-5-deoxy-5-(2-aminoethyl)amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

: 1432025-45-0
epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.cclet.2013.03.009

Reference yield:

: C₁₉H₂₃F₃N₁₂O₁₁S

: 1432025-45-0
epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.cclet.2013.03.009

Reference yield:

: 236115-80-3
1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine

: 1432025-45-0
epi-5-deoxy-5-[2-(6-hydroxynicotinyl)aminoethyl]amino-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetylneamine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 6 h / 20 °C / Inert atmosphere

2: pyridine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.cclet.2013.03.009