Vat Brown 1, Solubilised

Base Information

• Chemical Name: Vat Brown 1, Solubilised
• CAS No.: 23725-15-7
• Molecular Formula: C₈H₁₆O₄
• Molecular Weight: 176.213
• Mol file: 23725-15-7.mol

Synonyms:Dinaphtho[2,3-a:2',3'-i]naphth[2',3':6,7]indolo[2,3-c]carbazole-5,10,15,17,22,24-hexol,hexakis(hydrogen sulfate) (ester), hexasodium salt (8CI);Naphth[2',3':6,7]indolo[2,3-c]dinaphtho[2,3-a:2',3'-i]carbazole-5,10,15,17,22,24-hexol,hexakis(hydrogen sulfate) (ester), hexasodium salt (9CI); Ahcovat Soluble BrownIBR; Algosol Brown IBR-CF; Anthrasol Brown IBR; Arlindone Brown IBR; C.I.70801; C.I. Solubilised Vat Brown 1; C.I. Solubilised Vat Brown 1, hexasodiumsalt; Chemisol Brown BR; Cibantine Brown FBR; Daitosol Brown IBR; IndigosolBrown IBR; Mikethrene Soluble Brown IBR; Sandozol Brown BR; Solasol Brown BRS;Soledon Brown IBR; Soledon Dark Brown 3R; Solindolo Brown FBR; Soluble VatBrown BR; Solvat Brown BR; Tinosol Brown BR

Chemical Property of Vat Brown 1, Solubilised

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 473.58000
• Density: g/cm³
• LogP: 8.85920

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Vat Brown 1, Solubilised

There total 2 articles about Vat Brown 1, Solubilised which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

tert.-butylhydroperoxide (75-91-2) + isopropyl chloroformate (108-23-6) → OO-tert-butyl O-isopropyl monoperoxycarbonate (2372-21-6)

Guidance literature:

With potassium hydroxide; In water; at 19 - 31 ℃; Product distribution / selectivity;

Reference yield:

imidazolyl percarboxylate de t-butyle (69945-20-6) + isopropyl alcohol (67-63-0,8013-70-5) → dipercarbonate de O,O-t-butyle (3236-56-4) + OO-tert-butyl O-isopropyl monoperoxycarbonate (2372-21-6)

Guidance literature:

In tetrahydrofuran; Yield given; 1.) 0 deg C, 2.) rt, overnight;

upstream raw materials:

tert.-butylhydroperoxide

isopropyl chloroformate

imidazolyl percarboxylate de t-butyle

isopropyl alcohol

Refernces

• 1、 Bourgeois, Marie-Josephe,Campagnole, Monique,Filliatre, Claude,Maillard, Bernard,Villenave, Jean-Jaques. "Thermolyse en solution de percarbonates de O-alkyle et O,O-t-butyle". . p. 111 - 115. Retrieved 2007/10/02.