5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Base Information

Chemical Name:5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin
CAS No.:76196-49-1
Molecular Formula:C₆₀H₅₀N₄O₆
Molecular Weight:923.08
Hs Code.:

Synonyms:5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

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Chemical Property of 5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

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Technology Process of 5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

There total 7 articles about 5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 76196-48-0
5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

: 76196-49-1
5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Guidance literature:: With boron tribromide; In dichloromethane; at -80 ℃; for 5h;

Reference yield:

: 6202-39-7
homogentisic acid methyl ester dimethyl ether

: 76196-49-1
5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / conc. H₂SO₄ / CHCl₃; methanol / Heating; overnight

2: 65 percent / pyridine / Heating; overnight

3: 65 percent / boron tribromide / CH₂Cl₂ / 5 h / -80 °C

With pyridine; sulfuric acid; boron tribromide; In methanol; dichloromethane; chloroform;

Reference yield:

: 52711-92-9
2,5-dimethoxyphenylacetyl chloride

: 76196-49-1
5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / pyridine

2: 65 percent / pyridine / Heating; overnight

3: 65 percent / boron tribromide / CH₂Cl₂ / 5 h / -80 °C

With pyridine; boron tribromide; In dichloromethane;