5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Base Information

• Chemical Name: 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin
• CAS No.: 76196-48-0
• Molecular Formula: C₆₁H₅₂N₄O₆
• Molecular Weight: 937.107
• Mol file: 76196-48-0.mol

Synonyms:5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Chemical Property of 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin

There total 5 articles about 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

χ-hydroxypropyl 2,5-dimethoxyphenylacetate (76196-44-6) + 5-(p-benzoyl chloride)-10,15,20-tri(p-tolyl)porphyrin (61449-64-7) → 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin (76196-48-0)

Guidance literature:

With pyridine; Heating; overnight;

Reference yield:

homogentisic acid methyl ester dimethyl ether (6202-39-7) → 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin (76196-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 54 percent / conc. H₂SO₄ / CHCl₃; methanol / Heating; overnight

2: 65 percent / pyridine / Heating; overnight

With pyridine; sulfuric acid; In methanol; chloroform;

Reference yield:

(2,5-dimethoxyphenyl)acetic acid (1758-25-4) → 5-(p-benzoyloxypropyl 2,5-dimethoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin (76196-48-0)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / benzene / 3 h / Heating

2: 70 percent / pyridine

3: 65 percent / pyridine / Heating; overnight

With pyridine; thionyl chloride; In benzene;

upstream raw materials:

χ-hydroxypropyl 2,5-dimethoxyphenylacetate

5-(p-benzoyl chloride)-10,15,20-tri(p-tolyl)porphyrin

2,5-dimethoxyphenylacetyl chloride

(2,5-dimethoxyphenyl)acetic acid

Downstream raw materials:

5-(p-benzoyloxypropyl 2-hydroxy-5-methoxyphenylacetate)-10,15,20-tri(p-tolyl)porphyrin