2-propynyl salicylate

Base Information

• Chemical Name: 2-propynyl salicylate
• CAS No.: 13707-70-5
• Molecular Formula: C₁₀H₈O₃
• Molecular Weight: 176.172
• Mol file: 13707-70-5.mol

Synonyms:2-propynyl salicylate

Chemical Property of 2-propynyl salicylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-propynyl salicylate

There total 2 articles about 2-propynyl salicylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

propargyl alcohol (107-19-7) + salicylic acid (69-72-7,25496-36-0,8052-31-1) → 2-propynyl salicylate (13707-70-5)

Guidance literature:

In acetonitrile; for 24h; Reflux;

DOI:10.1039/d0cc02703k

Reference yield:

→ 2-propynyl salicylate (13707-70-5)

Guidance literature:

aus d. Hydroxysaeure durch Alkyl.;

Reference yield: 87.0%

2-propynyl salicylate (13707-70-5) + propargyl bromide (106-96-7) → prop-2-ynyl 2-(prop-2-ynyloxy)benzoate (14491-68-0)

Guidance literature:

2-propynyl salicylate; With potassium carbonate; In N,N-dimethyl-formamide; at 55 - 60 ℃; for 0.5h;

propargyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Further stages.;

DOI:10.1021/ol027382t

upstream raw materials:

propargyl alcohol

salicylic acid

Downstream raw materials:

prop-2-ynyl 2-(prop-2-ynyloxy)benzoate

prop-2-yn-1-yl 2-methoxybenzoate

salicylic acid