3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

Base Information

Chemical Name:3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine
CAS No.:122226-01-1
Molecular Formula:C₁₉H₃₃NO₃
Molecular Weight:323.476
Hs Code.:

Synonyms:3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

Chemical Property:

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Technology Process of 3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

There total 2 articles about 3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 116-11-0
2-Methoxypropene

: 104856-05-5,104856-06-6,114457-57-7,147373-31-7
(3RS,4S)-4-<(tert-butyloxy)carbonyl>-5-(cyclohexylmethyl)-3-hydroxy-1-pentene

: 122226-01-1
3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jm00168a009

Reference yield:

: 122226-01-1
3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

Guidance literature:

Reference yield:

: 122226-01-1
3-<(tert-butyloxy)carbonyl>-4-(cyclohexylmethyl)-2,2-dimethyl-5-vinyloxazolidine

: 127230-21-1
Toluene-4-sulfonic acid (2S,4S,5R,6S)-7-cyclohexyl-4,5-dihydroxy-2-methyl-6-(toluene-4-sulfonylamino)-heptyl ester

Guidance literature:: Multi-step reaction with 4 steps

2: 61 percent / Zn / tetrahydrofuran / 1 h / 50 °C

3: H₂ / 10percent Pd/C / methanol / 3040 Torr

4: 1.) 4 M HCl, EtOH, 2.) a) LiAlH₄ / 1.) dioxane, 30 min, 2.) a) THF, 0 deg C, 30 min, b) CHCl₃, reflux, 16 h

With hydrogenchloride; lithium aluminium tetrahydride; ethanol; hydrogen; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm00168a009