N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Base Information

Chemical Name:N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester
CAS No.:139657-19-5
Molecular Formula:C₃₂H₃₇N₃O₅
Molecular Weight:543.663
Hs Code.:

N-<N-<(tricyclo<3.3.1.1<sup>3,7</sup>>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Synonyms:N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

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Chemical Property of N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Chemical Property:

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Technology Process of N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

There total 3 articles about N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53120-53-9
2-adamantyl chloroformate

: 139657-19-5
N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaHCO₃, NaOH / dioxane / 18 h / Ambient temperature

2: 1.) N,N'-dicyclohexylcarbodiimide, 1-hydroxybenzotriazole monohydrate (HOBt) / 1.) CH₂Cl₂, 10 min, 2.) CH₂Cl₂, ethyl acetate, RT, 2 h

With sodium hydroxide; sodium hydrogencarbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00086a017

Reference yield:

: 153-94-6,27732-43-0,80206-30-0,27813-82-7
D-tryptophan

: 139657-19-5
N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaHCO₃, NaOH / dioxane / 18 h / Ambient temperature

2: 1.) N,N'-dicyclohexylcarbodiimide, 1-hydroxybenzotriazole monohydrate (HOBt) / 1.) CH₂Cl₂, 10 min, 2.) CH₂Cl₂, ethyl acetate, RT, 2 h

With sodium hydroxide; sodium hydrogencarbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00086a017

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 139657-07-1
tricyclo<3.3.1.1^3,7>dec-2-yl <1-carboxy-2-(1H-indol-3-yl)ethyl>carbamate

: 139657-19-5
N-3,7>dec-2-yloxy)carbonyl>-(R)-tryptophyl>-(S)-phenylalanine methyl ester

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) CH₂Cl₂, 10 min, 2.) CH₂Cl₂, ethyl acetate, RT, 2 h;
DOI:10.1021/jm00086a017