ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Base Information

Chemical Name:ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide
CAS No.:1373545-28-8
Molecular Formula:C₂₀H₂₃F₃N₂O₂S
Molecular Weight:412.476
Hs Code.:

Synonyms:ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Chemical Property of ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Technology Process of ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

There total 5 articles about ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373546-81-6
2-(4,4-dimethyl-6-(trifluoromethyl)-1,2,3,4-tetrahydroquinolin-2-yl)aniline

: 594-44-5
Ethanesulfonyl chloride

: 1373545-28-8
ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h; Cooling with ice; Inert atmosphere;

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1373545-28-8
ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / Reflux

2: boron trifluoride diethyl etherate / acetonitrile / 90 °C / sealed tube; Cooling with ice

3: ammonium chloride; iron / ethanol; water / 3 h / Inert atmosphere; Reflux

4: pyridine / dichloromethane / 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; iron; ammonium chloride; boron trifluoride diethyl etherate; In ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 1373545-28-8
ethanesulfonic acid [2-(4,4-dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / Reflux

2: boron trifluoride diethyl etherate / acetonitrile / 90 °C / sealed tube; Cooling with ice

3: ammonium chloride; iron / ethanol; water / 3 h / Inert atmosphere; Reflux

4: pyridine / dichloromethane / 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; iron; ammonium chloride; boron trifluoride diethyl etherate; In ethanol; dichloromethane; water; acetonitrile;