Benzol--imino-sulfonsaeurechlorid

Base Information

Chemical Name:Benzol--imino-sulfonsaeurechlorid
CAS No.:18506-87-1
Molecular Formula:C₉H₁₀ClNO₃S
Molecular Weight:247.702
Hs Code.:

Benzol-<N-carbethoxy>-imino-sulfonsaeurechlorid

Synonyms:Benzol--imino-sulfonsaeurechlorid

Suppliers and Price of Benzol--imino-sulfonsaeurechlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzol--imino-sulfonsaeurechlorid

Chemical Property:

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Technology Process of Benzol--imino-sulfonsaeurechlorid

There total 7 articles about Benzol--imino-sulfonsaeurechlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394013-23-0
ethyl phenylsulfinylcarbamate

: 18506-87-1
Benzol--imino-sulfonsaeurechlorid

Guidance literature:: With N-chloro-succinimide; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2012.06.072

Reference yield:

: 4972-29-6
benzenesulphinyl chloride

: 18506-87-1
Benzol--imino-sulfonsaeurechlorid

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.83 h / -78 - 20 °C

2.2: 20 °C / Saturated solution

3.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C

3.2: -78 - 20 °C

4.1: N-chloro-succinimide / acetonitrile / 2 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; n-butyllithium; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2012.06.072

Reference yield:

: 670-98-4
methyl benzenesulfinate

: 18506-87-1
Benzol--imino-sulfonsaeurechlorid

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.83 h / -78 - 20 °C

1.2: 20 °C / Saturated solution

2.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C

2.2: -78 - 20 °C

3.1: N-chloro-succinimide / acetonitrile / 2 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; n-butyllithium; lithium hexamethyldisilazane; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tet.2012.06.072