methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

Base Information

Chemical Name:methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate
CAS No.:1033726-45-2
Molecular Formula:C₁₄H₁₆N₂O₅
Molecular Weight:292.291
Hs Code.:

Synonyms:methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

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Chemical Property of methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

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Technology Process of methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

There total 1 articles about methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 13907-82-9,2650-67-1
N²-benzyloxycarbonyl-L-glutamine methyl ester

: 1033726-45-2
methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

Guidance literature:: N²-benzyloxycarbonyl-L-glutamine methyl ester; With [bis(acetoxy)iodo]benzene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

With water; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b801909f

Reference yield:

: 1033726-45-2
methyl 3-benzyloxycarbonyl-(tetrahydro)pyrimidin-2-one-4(S)-carboxylate

: (4R,6S)-4-Allyl-2-oxo-tetrahydro-pyrimidine-1,6-dicarboxylic acid 1-benzyl ester 6-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: electrochemical oxidation

2: TiCl₄

With titanium tetrachloride;
DOI:10.1051/jcp/1996930575