Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)-

Base Information

• Chemical Name: Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)-
• CAS No.: 75589-83-2
• Molecular Formula: C10H14NP
• Molecular Weight: 179.202
• DSSTox Substance ID: DTXSID10226496
• Nikkaji Number: J914.671G
• Wikidata: Q83105940
• Mol file: 75589-83-2.mol

Synonyms:Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)-;75589-83-2;DTXSID10226496

Chemical Property of Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)-

Chemical Property:

• XLogP3: 1.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 179.086386449
• Heavy Atom Count: 12
• Complexity: 157

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=PC1=CC=CC=C1)N(C)C

Technology Process of Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)-

There total 4 articles about Ethanamine, N,N-dimethyl-1-(phenylphosphinidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-Methoxy-1-phenylphosphanyl-ethyl)-dimethyl-amine (89865-20-3) → methanol (67-56-1) + N,N-dimethylamino-P-phenyl-C-methylmethylenephosphine (75589-83-2)

Guidance literature:

In acetonitrile; Heating;

DOI:10.1016/S0040-4039(00)81820-1

Reference yield:

N,N-dimethylacetamide dimethyl acetal (18871-66-4) + phenylphosphane (638-21-1) → N,N-dimethylamino-P-phenyl-C-methylmethylenephosphine (75589-83-2)

Guidance literature:

at 80 ℃; for 1h;

DOI:10.1016/S0040-4039(01)83934-4

Reference yield:

N,N-dimethylacetamide dimethyl acetal (18871-66-4) + phenylphosphane (638-21-1) → methanol (67-56-1) + N,N-dimethylamino-P-phenyl-C-methylmethylenephosphine (75589-83-2) + (1-Methoxy-1-phenylphosphanyl-ethyl)-dimethyl-amine (89865-20-3)

Guidance literature:

In acetonitrile; Heating;

DOI:10.1016/S0040-4039(00)81820-1

upstream raw materials:

(1-Methoxy-1-phenylphosphanyl-ethyl)-dimethyl-amine

N,N-dimethylacetamide dimethyl acetal

phenylphosphane

Downstream raw materials:

4-Cyanochlorobenzene

N,N-dimethyl acetamide

N¹,N¹-Dimethyl-N²-(phenyl)acetamidin