(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Base Information

Chemical Name:(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine
CAS No.:1352458-03-7
Molecular Formula:C₁₉H₂₇NO₂
Molecular Weight:301.429
Hs Code.:

Synonyms:(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Suppliers and Price of (E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

There total 3 articles about (E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1352457-92-1
(E)-4-(3,5-dimethoxystiryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridin-1-yloxyl

: 1352458-03-7
(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Guidance literature:: With iron; acetic acid; at 20 - 60 ℃; for 1h;
DOI:10.1016/j.bmc.2011.10.066

Reference yield:

: 40243-87-6
3,5-dimethoxystyrene

: 1352458-03-7
(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

2: iron; acetic acid / 1 h / 20 - 60 °C

With tetrabutylammomium bromide; palladium diacetate; iron; potassium carbonate; acetic acid; In N,N-dimethyl-formamide; 1: Heck reaction;
DOI:10.1016/j.bmc.2011.10.066

Reference yield:

: 78953-15-8
4-iodo-2,2,6,6-tetramethyl-3,6-dihydropyridin-1(2H)-yloxyl radical

: 1352458-03-7
(E)-4-(3,5-dimethoxystyryl)-2,2,6,6-tetramethyl-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

2: iron; acetic acid / 1 h / 20 - 60 °C

With tetrabutylammomium bromide; palladium diacetate; iron; potassium carbonate; acetic acid; In N,N-dimethyl-formamide; 1: Heck reaction;
DOI:10.1016/j.bmc.2011.10.066