N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

Base Information

Chemical Name:N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline
CAS No.:1214265-37-8
Molecular Formula:C₂₂H₂₂F₂N₂O₄
Molecular Weight:416.424
Hs Code.:

Synonyms:N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

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Chemical Property of N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

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Technology Process of N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

There total 4 articles about N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1214265-36-7
C₁₄H₁₆F₂N₂O₂

: 501-53-1,94274-21-2
benzyl chloroformate

: 1214265-37-8
N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; at 20 ℃; Ice bath;

Reference yield:

: 1214265-35-6
3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)-nitrobenzene

: 1214265-37-8
N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / tetrahydrofuran / 2 h / 2068.65 Torr

2: sodium hydrogencarbonate / water; acetone / 20 °C / Ice bath

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; water; acetone;

Reference yield:

: 129321-60-4
5,8-dioxa-10-azadispiro[2.0.44.33]undecane

: 1214265-37-8
N-carbobenzyloxy-[3,5-difluoro-4-(7,7-ethylenedioxy-5-azaspiro[2,4]heptan-5-yl)phenyl]aniline

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / Reflux

2: hydrogen / palladium on activated charcoal / tetrahydrofuran / 2 h / 2068.65 Torr

3: sodium hydrogencarbonate / water; acetone / 20 °C / Ice bath

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; water; acetone; acetonitrile;