tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate
CAS No.:1510865-67-4
Molecular Formula:C₁₅H₂₁N₃O₅S
Molecular Weight:355.415
Hs Code.:

Synonyms:tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

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Technology Process of tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

There total 2 articles about tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 398489-26-4
tert-butyl 3-oxoazetidine-1-carboxylate

: 1950-68-1
4-methoxybenzenesulfonyl hydrazide

: 1510865-67-4
tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

Guidance literature:: In toluene; for 2h; Reflux;

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 1510865-67-4
tert-butyl 3-(2-((4-methoxyphenyl)sulfonyl)hydrazineylidene)azetidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0 °C / Schlenk technique

2: dimethylsulfoxide-d6 / 60 °C / Schlenk technique

With hydrazine hydrate; In tetrahydrofuran; dimethylsulfoxide-d6;
DOI:10.1021/jo402526z