C₃₀H₅₀INO₃Si

Base Information

Chemical Name:C₃₀H₅₀INO₃Si
CAS No.:1072091-79-2
Molecular Formula:C₃₀H₅₀INO₃Si
Molecular Weight:627.722
Hs Code.:

C<sub>30</sub>H<sub>50</sub>INO<sub>3</sub>Si

Synonyms:C₃₀H₅₀INO₃Si

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Chemical Property of C₃₀H₅₀INO₃Si

Chemical Property:

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Technology Process of C₃₀H₅₀INO₃Si

There total 12 articles about C₃₀H₅₀INO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-38-3
C₁₇H₂₄INO

: 77744-45-7
7-((tert-butyldimethylsilyl)oxy)heptanoic acid

: 1072091-79-2
C₃₀H₅₀INO₃Si

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

: 1072091-14-5
tert-butyl {(1S,2E)-4-(benzyloxy)-1-[(1R)-2-hydroxy-1-methylethyl]-2-methylbut-2-en-1-yl}carbamate

: 1072091-79-2
C₃₀H₅₀INO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

2: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

3: hydrogenchloride / ethyl acetate / 1 h / 20 °C

4: triethylamine / dichloromethane / 3 h / 20 °C

5: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

6: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

7: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

With chromium dichloride; hydrogenchloride; lithium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; triethylamine; diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1072091-35-0
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-2-nitroaniline

: 1072091-79-2
C₃₀H₅₀INO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

2: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

With lithium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; mercaptoacetic acid; diisopropylamine; In N,N-dimethyl-formamide;