Technology Process of C18H24O5
There total 7 articles about C18H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate;
In
dichloromethane; water; acetone;
at 20 ℃;
for 0.25h;
DOI:10.1016/j.bmc.2011.02.053
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium iodide / acetone / 18 h / 60 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - -40 °C
2.2: 16 h / -78 - 20 °C
2.3: -78 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 50 °C / Inert atmosphere
4.1: camphor-10-sulfonic acid / 1,2-dichloro-ethane / 4 h / 20 °C
5.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
6.1: sodium dihydrogenphosphate; sodium chlorite / dichloromethane; water; acetone / 0.25 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; lithium aluminium tetrahydride; camphor-10-sulfonic acid; Dess-Martin periodane; sodium iodide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetone;
5.1: Dess-Martin oxidation / 6.1: Pannick oxidation;
DOI:10.1016/j.bmc.2011.02.053
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
2: sodium dihydrogenphosphate; sodium chlorite / dichloromethane; water; acetone / 0.25 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; Dess-Martin periodane;
In
dichloromethane; water; acetone;
1: Dess-Martin oxidation / 2: Pannick oxidation;
DOI:10.1016/j.bmc.2011.02.053
