N-<<(2R,4S)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

Base Information

Chemical Name:N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide
CAS No.:85199-40-2
Molecular Formula:C₂₁H₃₁NO₆
Molecular Weight:393.48
Hs Code.:

Synonyms:N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

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Chemical Property of N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

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Technology Process of N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

There total 3 articles about N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 535-17-1
2-acetoxypropionic acid

: 75099-07-9,85199-34-4
(2S,4R)-4-Benzyloxy-5,5-dimethyl-tetrahydro-pyran-2-carboximidic acid methyl ester

: 85199-40-2
N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1016/S0040-4020(01)86075-0

Reference yield:

: Acetic acid 1-{[1-((2S,4R)-4-benzyloxy-5,5-dimethyl-tetrahydro-pyran-2-yl)-1-methoxy-meth-(E)-ylidene]-carbamoyl}-ethyl ester

: 85199-40-2
Acetic acid 1-{[((2S,4R)-4-benzyloxy-5,5-dimethyl-tetrahydro-pyran-2-yl)-methoxy-methyl]-carbamoyl}-ethyl ester

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 0.25h; Yield given;
DOI:10.1016/S0040-4039(00)88691-8

Reference yield:

: 38939-83-2
2-acetoxypropionyl chloride

: 75099-07-9,85199-34-4
(2S,4R)-4-Benzyloxy-5,5-dimethyl-tetrahydro-pyran-2-carboximidic acid methyl ester

: 85199-40-2
N-<<(2R*,4S*)-4-(benzyloxy)tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-2-acetoxypropionamide

Guidance literature:: With pyridine; sodium tetrahydroborate; thionyl chloride; triethylamine; Multistep reaction; 1) CH₂Cl₂, 30 min. room temp.; 2) EtOH, -20 deg C, 20 min;
DOI:10.1016/S0040-4020(01)86075-0