N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide
CAS No.:147623-25-4
Molecular Formula:C₂₉H₃₂BrNO₄S
Molecular Weight:570.547
Hs Code.:

Synonyms:N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

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Chemical Property of N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

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Technology Process of N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

There total 5 articles about N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-39-0
benzyl bromide

: 147623-24-3
N-(2-Bromo-3-hydroxy-4-methoxy-5,6-dimethyl-phenyl)-N-cyclohex-2-enyl-4-methyl-benzenesulfonamide

: 147623-25-4
N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; for 16h;
DOI:10.1021/jo00061a017

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 147623-25-4
N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / pyridine / CH₂Cl₂ / 96 h

3: KOH / ethanol

4: 94 percent / aq. NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 16 h

With pyridine; potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; In ethanol; dichloromethane;
DOI:10.1021/jo00061a017

Reference yield:

: Acetic acid 3-amino-2-bromo-6-methoxy-4,5-dimethyl-phenyl ester

: 147623-25-4
N-<2-Bromo-4-methoxy-5,6-dimethyl-3-(phenylmethoxy)phenyl>-N-(2-cyclohexenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / pyridine / CH₂Cl₂ / 96 h

3: KOH / ethanol

4: 94 percent / aq. NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 16 h

With pyridine; potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; In ethanol; dichloromethane;
DOI:10.1021/jo00061a017