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4-bromo-N,β,β-trimethylphenylalanine

Base Information
  • Chemical Name:4-bromo-N,β,β-trimethylphenylalanine
  • CAS No.:676627-55-7
  • Molecular Formula:C12H16BrNO2
  • Molecular Weight:286.169
  • Hs Code.:
4-bromo-N,β,β-trimethylphenylalanine

Synonyms:4-bromo-N,β,β-trimethylphenylalanine

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Chemical Property of 4-bromo-N,β,β-trimethylphenylalanine
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Technology Process of 4-bromo-N,β,β-trimethylphenylalanine

There total 6 articles about 4-bromo-N,β,β-trimethylphenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
methylamine; 3-methyl-3-(4-bromophenyl)-2-oxobutanoic acid; In tetrahydrofuran; at 20 ℃; for 1h;
With borane pyridine; In tetrahydrofuran; Heating;
DOI:10.1021/ja048619e
Guidance literature:
With borane pyridine; In tetrahydrofuran; at 45 - 55 ℃;
DOI:10.1021/jm040056u
Guidance literature:
Multi-step reaction with 2 steps
1.1: 79 percent / bromine; iron / CCl4 / Heating
2.1: tetrahydrofuran / 1 h / 20 °C
2.2: 49 percent / BH3*pyridine / tetrahydrofuran / Heating
With bromine; iron; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/ja048619e
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