3'-nitrobiphenyl-3-quinoline carboxylate

Base Information

Chemical Name:3'-nitrobiphenyl-3-quinoline carboxylate
CAS No.:223102-43-0
Molecular Formula:C₂₃H₁₆N₂O₄
Molecular Weight:384.391
Hs Code.:

Synonyms:3'-nitrobiphenyl-3-quinoline carboxylate

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Chemical Property of 3'-nitrobiphenyl-3-quinoline carboxylate

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Technology Process of 3'-nitrobiphenyl-3-quinoline carboxylate

There total 3 articles about 3'-nitrobiphenyl-3-quinoline carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 13331-27-6
m-nitrobenzene boronic acid

: 223102-42-9
3-bromobenzyl-3-quinoline carboxylate

: 223102-43-0
3'-nitrobiphenyl-3-quinoline carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; at 75 ℃; for 4h;
DOI:10.1021/jo9809074

Reference yield:

: 6480-68-8
quinoline-3-carboxylic acid

: 223102-43-0
3'-nitrobiphenyl-3-quinoline carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride, DMAP / CH₂Cl₂ / 3 h / Ambient temperature

2: 83 percent / Pd(PPh₃)4, Na₂CO₃ / 1,2-dimethoxy-ethane / 4 h / 75 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jo9809074

Reference yield:

: 15852-73-0
(3-Bromophenyl)methanol

: 223102-43-0
3'-nitrobiphenyl-3-quinoline carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride, DMAP / CH₂Cl₂ / 3 h / Ambient temperature

2: 83 percent / Pd(PPh₃)4, Na₂CO₃ / 1,2-dimethoxy-ethane / 4 h / 75 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jo9809074