C₆H₁₁P(C₃H₆P(OCH₃)2)2

Base Information

Chemical Name:C₆H₁₁P(C₃H₆P(OCH₃)2)2
CAS No.:850716-21-1
Molecular Formula:C₁₆H₃₅O₄P₃
Molecular Weight:384.373
Hs Code.:

C<sub>6</sub>H<sub>11</sub>P(C<sub>3</sub>H<sub>6</sub>P(OCH<sub>3</sub>)2)2

Synonyms:C₆H₁₁P(C₃H₆P(OCH₃)2)2

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Chemical Property of C₆H₁₁P(C₃H₆P(OCH₃)2)2

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Technology Process of C₆H₁₁P(C₃H₆P(OCH₃)2)2

There total 1 articles about C₆H₁₁P(C₃H₆P(OCH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 822-68-4
cyclohexylphosphine

: dimethylallylphosphonite

: 850716-21-1
C₆H₁₁P(C₃H₆P(OCH₃)2)2

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 20 ℃; for 48h; Irradiation;
DOI:10.1016/j.jorganchem.2004.11.055

Reference yield: 71.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 850716-21-1
C₆H₁₁P(C₃H₆P(OCH₃)2)2

: 850715-87-6
[Ru(C₆H₁₁P(C₃H₆P(OCH₃)2)2)(CO)2]

Guidance literature:: In toluene; byproducts: CO; (N2); glovebox or Schlenk technique; phosphine was added to soln. of Ru complex in toluene; mixt. was heated to 40°C for 4 h; refluxed for 4 d; NMR monitoring; toluene removed (vac.); extd. (pentane); filtered over Celite; recrystd. (toluene/pentane, -30°C); elem. anal.;
DOI:10.1016/j.jorganchem.2004.11.055

Reference yield: 28.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 850716-21-1
C₆H₁₁P(C₃H₆P(OCH₃)2)2

: 850715-91-2
[Fe(C₆H₁₁P(C₃H₆P(OCH₃)2)2)(CO)2]

Guidance literature:: In benzene; Irradiation (UV/VIS); (N2); glovebox or Schlenk technique; mixt. of phosphine and Fe complex in C6H6 was irradiated with stirring at room temp. for 5 h; C6H6 removed (vac); chromd. (C6H6/THF); recrystd. (toluene/pentane, -30°C); elem. anal.;
DOI:10.1016/j.jorganchem.2004.11.055