(E)-3-nitro-4'-acetoazobenzene

Base Information

• Chemical Name: (E)-3-nitro-4'-acetoazobenzene
• CAS No.: 106782-72-3
• Molecular Formula: C₁₄H₁₁N₃O₃
• Molecular Weight: 269.26
• Mol file: 106782-72-3.mol

Synonyms:(E)-3-nitro-4'-acetoazobenzene

Chemical Property of (E)-3-nitro-4'-acetoazobenzene

Chemical Property:

Purity/Quality:

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Technology Process of (E)-3-nitro-4'-acetoazobenzene

There total 1 articles about (E)-3-nitro-4'-acetoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-nitro-3-nitrosobenzene (17122-21-3) + p-aminobenzophenone (99-92-3) → (E)-3-nitro-4'-acetoazobenzene (106782-72-3)

Guidance literature:

With acetic acid; at 20 ℃; for 12h; Sonication;

DOI:10.3762/bjoc.8.209

Reference yield: 73.0%

(E)-3-nitro-4'-acetoazobenzene (106782-72-3) → (E)-3-amino-4’-acetoazobenzene (1417805-64-1)

Guidance literature:

With 10% Pd/C; hydrogen; In methanol; at 20 ℃; for 4h;

DOI:10.3762/bjoc.8.209

upstream raw materials:

1-nitro-3-nitrosobenzene

p-aminobenzophenone

Downstream raw materials:

(E)-3-amino-4’-acetoazobenzene