ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside
CAS No.:151992-84-6
Molecular Formula:C₃₀H₃₂O₇S
Molecular Weight:536.646
Hs Code.:

Synonyms:ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 98-88-4
benzoyl chloride

: 151992-83-5
ethyl 3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

: 151992-84-6
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(93)84030-A

Reference yield: 70.0%

: 151992-84-6
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

: 151992-85-7
ethyl 2-O-benzoyl-3-O-benzyl-4-O-(4-methoxybenzyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With chloro-trimethyl-silane; molecular sieve; sodium cyanoborohydride; In acetonitrile; for 6h; Ambient temperature;
DOI:10.1016/0008-6215(93)84030-A

Reference yield:

: 151992-84-6
ethyl 2-O-benzoyl-3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

: 151992-86-8
tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Me₃SiCl, NaCNBH₃, molecular sieves / acetonitrile / 6 h / Ambient temperature

2: 68 percent / pyridinium dichromate, Ac₂O / CH₂Cl₂ / 6 h / Ambient temperature

With dipyridinium dichromate; chloro-trimethyl-silane; molecular sieve; acetic anhydride; sodium cyanoborohydride; In dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(93)84030-A