tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Base Information

Chemical Name:tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate
CAS No.:151992-86-8
Molecular Formula:C₃₄H₄₀O₈S
Molecular Weight:608.753
Hs Code.:

Synonyms:tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Suppliers and Price of tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

There total 4 articles about tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 151992-85-7
ethyl 2-O-benzoyl-3-O-benzyl-4-O-(4-methoxybenzyl)-1-thio-β-D-glucopyranoside

: 75-65-0
tert-butyl alcohol

: 151992-86-8
tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Guidance literature:: With dipyridinium dichromate; acetic anhydride; In dichloromethane; for 6h; Ambient temperature;
DOI:10.1016/0008-6215(93)84030-A

Reference yield:

: 98-88-4
benzoyl chloride

: 151992-86-8
tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 70 percent / Me₃SiCl, NaCNBH₃, molecular sieves / acetonitrile / 6 h / Ambient temperature

3: 68 percent / pyridinium dichromate, Ac₂O / CH₂Cl₂ / 6 h / Ambient temperature

With pyridine; dipyridinium dichromate; chloro-trimethyl-silane; molecular sieve; acetic anhydride; sodium cyanoborohydride; In dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(93)84030-A

Reference yield:

: 151992-83-5
ethyl 3-O-benzyl-4,6-O-p-methoxybenzylidene-1-thio-β-D-glucopyranoside

: 151992-86-8
tert-butyl (ethyl 2-O-benzoyl-3-O-benzyl-4-O-p-methoxybenzyl-1-thio-β-D-glucopyranosid)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 70 percent / Me₃SiCl, NaCNBH₃, molecular sieves / acetonitrile / 6 h / Ambient temperature

3: 68 percent / pyridinium dichromate, Ac₂O / CH₂Cl₂ / 6 h / Ambient temperature

With pyridine; dipyridinium dichromate; chloro-trimethyl-silane; molecular sieve; acetic anhydride; sodium cyanoborohydride; In dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(93)84030-A