2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

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Chemical Name:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate
CAS No.:1439365-39-5
Molecular Formula:C₄₅H₆₀N₆O₈
Molecular Weight:813.007
Hs Code.:

Synonyms:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

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Chemical Property of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

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Technology Process of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

There total 9 articles about 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1439365-38-4
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

: 1439365-39-5
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

Guidance literature:: With 2,6-di-tert-butylphenol; triethylamine; In dichloromethane;

Reference yield:

: 111-83-1
1-bromo-octane

: 1439365-39-5
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium oxide / water / 48 h / 110 °C

2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1.5 h / 5 - 40 °C

2.2: 20 °C / Cooling with ice

3.1: lithium hydroxide / tetrahydrofuran / 20 °C

4.1: potassium carbonate / dichloromethane / 20 - 35 °C

5.1: triethylamine; 2,6-di-tert-butylphenol / dichloromethane

With nitrosylsulfuric acid; 2,6-di-tert-butylphenol; magnesium oxide; potassium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; water;

Reference yield:

: 1439365-36-2
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl)diacetate

: 1439365-39-5
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)bis( ethane-2, 1-diyl)diacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / tetrahydrofuran / 20 °C

2: potassium carbonate / dichloromethane / 20 - 35 °C

3: triethylamine; 2,6-di-tert-butylphenol / dichloromethane

With 2,6-di-tert-butylphenol; potassium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane;