2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Chemical Name:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)
CAS No.:1439365-38-4
Molecular Formula:C₄₅H₆₂Cl₂N₆O₈
Molecular Weight:885.929
Hs Code.:

Synonyms:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Chemical Property of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Technology Process of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

There total 8 articles about 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1439365-37-3
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

: 625-36-5
2-chloropropionyl chloride

: 1439365-38-4
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 - 35 ℃;

Reference yield:

: 111-83-1
1-bromo-octane

: 1439365-38-4
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium oxide / water / 48 h / 110 °C

2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1.5 h / 5 - 40 °C

2.2: 20 °C / Cooling with ice

3.1: lithium hydroxide / tetrahydrofuran / 20 °C

4.1: potassium carbonate / dichloromethane / 20 - 35 °C

With nitrosylsulfuric acid; magnesium oxide; potassium carbonate; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; water;

Reference yield:

: 1439365-36-2
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl)diacetate

: 1439365-38-4
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran / 20 °C

2: potassium carbonate / dichloromethane / 20 - 35 °C

With potassium carbonate; lithium hydroxide; In tetrahydrofuran; dichloromethane;