2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

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Chemical Name:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol
CAS No.:1439365-37-3
Molecular Formula:C₃₉H₅₆N₆O₆
Molecular Weight:704.91
Hs Code.:

Synonyms:2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

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Chemical Property of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

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Technology Process of 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

There total 7 articles about 2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1439365-36-2
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl)diacetate

: 1439365-37-3
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 57154-24-2
3-methyl-N,N-dioctylaniline

: 1439365-37-3
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1.5 h / 5 - 40 °C

1.2: 20 °C / Cooling with ice

2.1: lithium hydroxide / tetrahydrofuran / 20 °C

With nitrosylsulfuric acid; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;

Reference yield:

: 187960-21-0
2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

: 1439365-37-3
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1.5 h / 5 - 40 °C

1.2: 20 °C / Cooling with ice

2.1: lithium hydroxide / tetrahydrofuran / 20 °C

With nitrosylsulfuric acid; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;