C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

Base Information

Chemical Name:C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)
CAS No.:804530-53-8
Molecular Formula:C₁₆H₂₆N₂Zn
Molecular Weight:311.786
Hs Code.:

C<sub>2</sub>H<sub>5</sub>CHC(C<sub>6</sub>H<sub>5</sub>)N(N(CH<sub>3</sub>)2)Zn(C(CH<sub>3</sub>)3)

Synonyms:C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

Chemical Property:

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Technology Process of C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

There total 2 articles about C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19679-59-5
propiophenone N,N-dimethylhydrazone

: 594-19-4
tert.-butyl lithium

: 7646-85-7,24359-56-6
zinc(II) chloride

: 804530-53-8
C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

Guidance literature:: With tert-butyllithium; In diethyl ether; byproducts: LiCl; hydrazone was treated with 1 equiv of tert-butyllithium followed by addn. of 1 equiv of anhydrous ZnCl2 in ether; solvent was removed in vac.;
DOI:10.1021/ja806258v

Reference yield:

: 594-19-4
tert.-butyl lithium

: 33785-78-3
N,N-dimethylhydrazone of 1-phenylbutan-1-one

: 7646-85-7,24359-56-6
zinc(II) chloride

: 804530-53-8
C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

Guidance literature:: In not given; hydrazone was treated with t-BuLi (2 equiv.); ZnCl2 (1 equiv.) was added;
DOI:10.1021/ja044878s

Reference yield: 80.0%

: 804530-53-8
C₂H₅CHC(C₆H₅)N(N(CH₃)2)Zn(C(CH₃)3)

: 106-95-6
allyl bromide

: 126688-97-9
2-[(1E)-hex-1-en-1-yl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: OC(CH₃)2C(CH₃)2OBCH(CH₂CHCH₂)CH(C₄H₉)CH(C₂H₅)C(C₆H₅)N(N(CH₃)2)

Guidance literature:: With copper(l) chloride; In hexane; Zn compd. (1.25 equiv.) and B compd. (1 equiv.) were reacted in hexane at 0°C for 12-48 h; treated with bromide (2-4 equiv.) in Et2O in presence of CuCl (1-2 equiv.);
DOI:10.1021/ja044878s