2-Dicyanomethylene-5-phenyladamantane

Base Information

• Chemical Name: 2-Dicyanomethylene-5-phenyladamantane
• CAS No.: 250637-43-5
• Molecular Formula: C₁₉H₁₈N₂
• Molecular Weight: 274.365
• Mol file: 250637-43-5.mol

Synonyms:2-Dicyanomethylene-5-phenyladamantane

Chemical Property of 2-Dicyanomethylene-5-phenyladamantane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-Dicyanomethylene-5-phenyladamantane

There total 1 articles about 2-Dicyanomethylene-5-phenyladamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-phenyladamantan-2-one (38584-33-7) + malononitrile (109-77-3) → 2-Dicyanomethylene-5-phenyladamantane (250637-43-5)

Guidance literature:

With ammonium acetate; In ethanol; at 20 ℃;

DOI:10.1039/a901484e

Reference yield: 60.0%

phenylmagnesium bromide + 2-Dicyanomethylene-5-phenyladamantane (250637-43-5) → 2-Dibenzoylmethylene-5-phenyladamantane

Guidance literature:

phenylmagnesium bromide; 2-Dicyanomethylene-5-phenyladamantane; In diethyl ether; at 20 ℃; for 0.5h;

With hydrogenchloride; water; In diethyl ether;

DOI:10.1039/a901484e

Reference yield:

methyl magnesium iodide (917-64-6) + 2-Dicyanomethylene-5-phenyladamantane (250637-43-5) → (Z)-2-Methyl-2-dicyanomethyl-5-phenyladamantane + (E)-2-Methyl-2-dicyanomethyl-5-phenyladamantane

Guidance literature:

In diethyl ether; at 20 ℃;

DOI:10.1039/a901484e

upstream raw materials:

5-phenyladamantan-2-one

malononitrile

Refernces