N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

Base Information

Chemical Name:N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide
CAS No.:862132-81-8
Molecular Formula:C₁₉H₁₅F₇N₂O₃
Molecular Weight:452.329
Hs Code.:

Synonyms:N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

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Chemical Property of N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

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Technology Process of N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

There total 3 articles about N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 847622-53-1
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide

: 74-88-4
methyl iodide

: 862132-81-8
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

Guidance literature:: N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-3-nitrobenzamide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 50 ℃; for 4h;

Reference yield:

: 273735-43-6
4-heptafluoroisopropyl-2,6-dimethylaniline

: 862132-81-8
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / tetrahydrofuran / 10 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: 4 h / 50 °C

With pyridine; sodium hydride; In tetrahydrofuran;

Reference yield:

: 121-90-4
m-nitrobenzoic acid chloride

: 862132-81-8
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-N-methyl-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / tetrahydrofuran / 10 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: 4 h / 50 °C

With pyridine; sodium hydride; In tetrahydrofuran;