C₂₀H₂₃BrN₂O₃

Base Information

Chemical Name:C₂₀H₂₃BrN₂O₃
CAS No.:1228311-79-2
Molecular Formula:C₂₀H₂₃BrN₂O₃
Molecular Weight:419.318
Hs Code.:

C<sub>20</sub>H<sub>23</sub>BrN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₀H₂₃BrN₂O₃

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Chemical Property of C₂₀H₂₃BrN₂O₃

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Technology Process of C₂₀H₂₃BrN₂O₃

There total 4 articles about C₂₀H₂₃BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 64-17-5
ethanol

: C₁₈H₁₉BrN₂O₃

: 1228311-79-2
C₂₀H₂₃BrN₂O₃

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.3762/bjoc.8.55

Reference yield:

: 105299-45-4,2497-38-3
4-(4-hydroxphenylazo)benzoic acid

: 1228311-79-2
C₂₀H₂₃BrN₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / ethanol / 20 h / Reflux; Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In ethanol; dichloromethane;
DOI:10.3762/bjoc.8.55

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1228311-79-2
C₂₀H₂₃BrN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; sodium nitrite / 1 h / 0 °C

2: potassium carbonate; potassium iodide / ethanol / 20 h / Reflux; Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; sodium nitrite; In ethanol; dichloromethane;
DOI:10.3762/bjoc.8.55