N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

Base Information

• Chemical Name: N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide
• CAS No.: 213123-43-4
• Molecular Formula: C₂₁H₂₄N₂O₅
• Molecular Weight: 384.432

Synonyms:N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

Chemical Property of N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

There total 6 articles about N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-((2R,4aR,6S,7S,8S,8aS)-7-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide (213123-42-3) → N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide (213123-43-4)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; under 760 Torr; Ambient temperature;

DOI:10.1016/S0968-0896(98)00027-3

Reference yield:

benzoic acid anhydride (93-97-0) → N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide (213123-43-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 89.8 percent / pyridine / 0.5 h

2: 70 percent / NaN₃, NH₄Cl / dimethylformamide / 120 °C

3: 1 g / H₂, HCl / 10percent palladium on charcoal / methanol / 760 Torr / Ambient temperature

With hydrogenchloride; sodium azide; hydrogen; ammonium chloride; palladium on activated charcoal; In pyridine; methanol; N,N-dimethyl-formamide;

DOI:10.1016/S0968-0896(98)00027-3

Reference yield:

methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-α-D-allopyranoside (71184-91-3) → N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide (213123-43-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 89.8 percent / pyridine / 0.5 h

2: 70 percent / NaN₃, NH₄Cl / dimethylformamide / 120 °C

3: 1 g / H₂, HCl / 10percent palladium on charcoal / methanol / 760 Torr / Ambient temperature

With hydrogenchloride; sodium azide; hydrogen; ammonium chloride; palladium on activated charcoal; In pyridine; methanol; N,N-dimethyl-formamide;

DOI:10.1016/S0968-0896(98)00027-3

upstream raw materials:

N-((2R,4aR,6S,7S,8S,8aS)-7-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-α-D-allopyranoside

methyl 2-N-benzoylamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

(+)-D-glucosamine hydrochloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 213123-43-4 N-((2R,4aR,6S,7S,8S,8aS)-7-Amino-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-benzamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send