p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside
CAS No.:1381875-99-5
Molecular Formula:C₄₈H₅₀O₁₁Si
Molecular Weight:831.004
Hs Code.:

Synonyms:p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

There total 3 articles about p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1381875-87-1
p-methoxyphenyl 2,3-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1381875-99-5
p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2012.02.021

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1381875-99-5
p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; 1H-imidazole / 0 - 20 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.carres.2012.02.021

Reference yield:

: 1200878-78-9
p-methoxyphenyl 2,3-di-O-benzoyl-β-D-glucopyranoside

: 1381875-99-5
p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; 1H-imidazole / 0 - 20 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.carres.2012.02.021