p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside
CAS No.:1381876-01-2
Molecular Formula:C₃₂H₃₂O₁₁
Molecular Weight:592.599
Hs Code.:

Synonyms:p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

There total 10 articles about p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1200878-78-9
p-methoxyphenyl 2,3-di-O-benzoyl-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1381876-01-2
p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: p-methoxyphenyl 2,3-di-O-benzoyl-β-D-glucopyranoside; levulinic acid; With 2-chloro-1-methyl-pyridinium iodide; In chloroform; 1,2-dichloro-ethane; at 20 ℃; for 0.333333h;

With 1,4-diaza-bicyclo[2.2.2]octane; In chloroform; 1,2-dichloro-ethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo4012442

Reference yield: 71.0%

: 1381875-99-5
p-methoxyphenyl 2,3-di-O-benzoyl-4-O-levulinoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

: 1381876-01-2
p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: With perchloric acid on silica gel; In acetonitrile; at 50 ℃; for 3h; chemoselective reaction;
DOI:10.1016/j.carres.2012.02.021

Reference yield:

: 1200878-78-9
p-methoxyphenyl 2,3-di-O-benzoyl-β-D-glucopyranoside

: 1381876-01-2
p-methoxyphenyl 2,3-di-O-benzoyl-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; 1H-imidazole / 0 - 20 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

3: perchloric acid on silica gel / acetonitrile / 3 h / 50 °C

With pyridine; 1H-imidazole; dmap; perchloric acid on silica gel; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2012.02.021