(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

Base Information

Chemical Name:(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}
CAS No.:949087-01-8
Molecular Formula:C₂₂H₃₁N₃O₇
Molecular Weight:449.504
Hs Code.:

Synonyms:(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

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Chemical Property of (+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

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Technology Process of (+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

There total 6 articles about (+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 949087-01-8
(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

Guidance literature:: Multi-step reaction with 4 steps

1: 2.32 g / ethanol / 24 h / 20 °C

2: 84 percent / dimethylformamide / 100 °C

3: hydrazine hydrate / methanol / 3 h / Heating

4: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

With dmap; hydrazine hydrate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 22323-82-6,36543-79-0
(S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol

: 949087-01-8
(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

Guidance literature:: Multi-step reaction with 3 steps

1: KMnO₄; KOH / H₂O / 14 h / 20 °C

2: pyridine; (ClCO)2 / diethyl ether / 14 h / 20 °C

3: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

With pyridine; dmap; potassium hydroxide; potassium permanganate; oxalyl dichloride; triethylamine; In diethyl ether; dichloromethane; water;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 114746-70-2,62075-55-2
(R)-2,2-dimethyl-[1,3]dioxolane-4-carboxylic acid

: 949087-01-8
(+)-N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis{[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]carboxamide}

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; (ClCO)2 / diethyl ether / 14 h / 20 °C

2: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

With pyridine; dmap; oxalyl dichloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2007.05.109