N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

Base Information

Chemical Name:N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]
CAS No.:949087-06-3
Molecular Formula:C₃₀H₃₅N₃O₇
Molecular Weight:549.624
Hs Code.:

Synonyms:N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

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Chemical Property of N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

Chemical Property:

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Technology Process of N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

There total 6 articles about N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 949087-05-2
N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}-bis[(2R)-2,3-dihydroxypropanamide]

: 100-39-0
benzyl bromide

: 949087-06-3
N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

Guidance literature:: N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}-bis[(2R)-2,3-dihydroxypropanamide]; With di(n-butyl)tin oxide; In methanol; toluene; Heating;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In methanol; toluene; for 5h; Further stages.; Heating;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 949087-06-3
N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2.32 g / ethanol / 24 h / 20 °C

2.1: 84 percent / dimethylformamide / 100 °C

3.1: hydrazine hydrate / methanol / 3 h / Heating

4.1: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

5.1: 100 percent / D,L-camphorsulfonic acid / ethanol / 3 h / Heating

6.1: di-n-butyltin oxide / toluene; methanol / Heating

6.2: 34 percent / tetrabutylammonium iodide / methanol; toluene / 5 h / Heating

With dmap; camphor-10-sulfonic acid; di(n-butyl)tin oxide; hydrazine hydrate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 949086-96-8
2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

: 949087-06-3
N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis[(2R)-3-(benzyloxy)-2-hydroxypropanamide]

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / methanol / 3 h / Heating

2.1: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

3.1: 100 percent / D,L-camphorsulfonic acid / ethanol / 3 h / Heating

4.1: di-n-butyltin oxide / toluene; methanol / Heating

4.2: 34 percent / tetrabutylammonium iodide / methanol; toluene / 5 h / Heating

With dmap; camphor-10-sulfonic acid; di(n-butyl)tin oxide; hydrazine hydrate; triethylamine; In methanol; ethanol; dichloromethane; toluene;
DOI:10.1016/j.tet.2007.05.109