N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

Base Information

• Chemical Name: N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester
• CAS No.: 222853-54-5
• Molecular Formula: C₂₄H₃₀N₄O₆
• Molecular Weight: 470.525

Synonyms:N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

Chemical Property of N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

Chemical Property:

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Technology Process of N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

There total 2 articles about N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

3-propanamide (133382-98-6) + phenyl chloroformate (1885-14-9) → N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester (222853-54-5)

Guidance literature:

With triethylamine; In methanol;

DOI:10.1016/S0960-894X(99)00049-9

Reference yield:

(S)-tert-butyl (1-hydrazinyl-1-oxo-3-phenylpropan-2-yl)carbamate (30189-48-1) → N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester (222853-54-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / dimethylformamide / 36 h / 110 °C

2: 70 percent / Et₃N / methanol

With triethylamine; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(99)00049-9

Reference yield:

N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester (222853-54-5) → N'-(2-amino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1016/S0960-894X(99)00049-9

upstream raw materials:

3-propanamide

phenyl chloroformate

(S)-tert-butyl (1-hydrazinyl-1-oxo-3-phenylpropan-2-yl)carbamate

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