benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

Base Information

Chemical Name:benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate
CAS No.:1256922-16-3
Molecular Formula:C₂₂H₂₄N₄O₅
Molecular Weight:424.456
Hs Code.:

Synonyms:benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

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Technology Process of benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

There total 2 articles about benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1123-44-0
3-amino-5,5'-dimethylimidazolidine-2,4-dione

: 1161-13-3
N-Cbz-L-Phe

: 1256922-16-3
benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.crci.2010.01.011

Reference yield:

: 77-71-4
5,5-dimethyl-imidazolidine-2,4-dione

: 1256922-16-3
benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate

2: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.crci.2010.01.011

Reference yield: 75.0%

: 1256922-16-3
benzyl 1-(4,4-dimethyl-2,5-dioxoimidazolidin-1-ylcarbamoyl)-2-phenylethylcarbamate

: 1256922-19-6
2-amino-N-(4,4-dimethyl-2,5-dioxoimidazolidin-1-yl)-3-phenylpropanamide

Guidance literature:: With hydrogenchloride; palladium on activated charcoal; hydrogen; In methanol; water; at 20 ℃; for 5h;
DOI:10.1016/j.crci.2010.01.011