(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

Base Information

Chemical Name:(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate
CAS No.:1370348-26-7
Molecular Formula:C₁₉H₂₉NO₆S₂
Molecular Weight:431.574
Hs Code.:

Synonyms:(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

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Chemical Property of (S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

Chemical Property:

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Technology Process of (S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

There total 7 articles about (S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.2%

: 1370348-25-6
(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

: 10387-40-3
potassium thioacetate

: 1370348-26-7
(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

Guidance literature:: In acetone; at 20 ℃; for 2h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1370348-26-7
(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / water; tetrahydrofuran / 5 - 20 °C

2: thionyl chloride / 1 h / 50 °C

3: sulfuryl dichloride / ethanol / 5 - 10 °C

4: triethylamine / toluene / 0 - 20 °C

5: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

6: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

7: acetone / 2 h / 20 °C

With lithium borohydride; thionyl chloride; sulfuryl dichloride; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; acetone; toluene;

Reference yield:

: 149835-71-2
(2S,2S') diethyl 4,4'-disulfanediylbis(2-(benzyloxycarbonylamino)butanoate)

: 1370348-26-7
(S) 2-(benzyloxycarbonylamino) 4-(neopentyloxysulfonyl)butyl thioacetate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuryl dichloride / ethanol / 5 - 10 °C

2: triethylamine / toluene / 0 - 20 °C

3: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

4: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

5: acetone / 2 h / 20 °C

With lithium borohydride; sulfuryl dichloride; triethylamine; In tetrahydrofuran; ethanol; tert-butyl methyl ether; acetone; toluene;