(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

Base Information

Chemical Name:(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate
CAS No.:1370348-25-6
Molecular Formula:C₁₈H₂₉NO₈S₂
Molecular Weight:451.562
Hs Code.:

Synonyms:(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

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Chemical Property of (S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

Chemical Property:

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Technology Process of (S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

There total 6 articles about (S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 1370348-24-5
(S)-neopentyl 3-(benzyloxycarbonylamino) 4-hydroxybutane 1-sulfonate

: 124-63-0
methanesulfonyl chloride

: 1370348-25-6
(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

Guidance literature:: With triethylamine; In tert-butyl methyl ether; toluene; at 10 - 20 ℃;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1370348-25-6
(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / water; tetrahydrofuran / 5 - 20 °C

2: thionyl chloride / 1 h / 50 °C

3: sulfuryl dichloride / ethanol / 5 - 10 °C

4: triethylamine / toluene / 0 - 20 °C

5: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

6: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

With lithium borohydride; thionyl chloride; sulfuryl dichloride; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; toluene;

Reference yield:

: 149835-71-2
(2S,2S') diethyl 4,4'-disulfanediylbis(2-(benzyloxycarbonylamino)butanoate)

: 1370348-25-6
(S)-neopentyl 3-(benzyloxycarbonylamino) 4-(methylsulfonyloxy)butane 1-sulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuryl dichloride / ethanol / 5 - 10 °C

2: triethylamine / toluene / 0 - 20 °C

3: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

4: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

With lithium borohydride; sulfuryl dichloride; triethylamine; In tetrahydrofuran; ethanol; tert-butyl methyl ether; toluene;