S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

Base Information

Chemical Name:S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate
CAS No.:959161-41-2
Molecular Formula:C₁₂H₁₅NO₄S
Molecular Weight:269.321
Hs Code.:

Synonyms:S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

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Chemical Property of S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

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Technology Process of S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

There total 3 articles about S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14922-36-2
4-nitrophenylglyoxylic acid

: 959161-41-2
S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / CH₂Cl₂ / 0.5 h / cooling

2: triethylamine / CH₂Cl₂ / 0 - 20 °C

3: sodium borohydride / tetrahydrofuran

With sodium tetrahydroborate; oxalyl dichloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo070575f

Reference yield:

: 57699-27-1
methyl p-nitrophenylglyoxylate

: 959161-41-2
S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / H₂O; ethanol

2: oxalyl chloride / CH₂Cl₂ / 0.5 h / cooling

3: triethylamine / CH₂Cl₂ / 0 - 20 °C

4: sodium borohydride / tetrahydrofuran

With potassium hydroxide; sodium tetrahydroborate; oxalyl dichloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jo070575f

Reference yield:

: 105248-77-9
4-nitro-α-oxophenylacetyl chloride

: 959161-41-2
S-t-butyl hydroxy-(4-nitrophenyl)-thioacetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 0 - 20 °C

2: sodium borohydride / tetrahydrofuran

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo070575f