iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

Base Information

Chemical Name:iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride
CAS No.:99688-17-2
Molecular Formula:C₄₈H₃₄ClFeN₄O₂
Molecular Weight:790.124
Hs Code.:

Synonyms:iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

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Chemical Property of iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

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Technology Process of iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

There total 1 articles about iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: ferrous(II) sulfate heptahydrate

: 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin

: 99688-17-2
iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

Guidance literature:: With pyridine; hydrogenchloride; In water; acetic acid; porphyrin dissolved in glacial CH3COOH under N2 and heated to 85°C, C5H5N and FeSO4*7H2O (satd. aq. soln.) added, heated for 30 min, cooled, H2O added; Fe porphyrin collected by filtration, washed with H2O, chromd. (SiO2, CHCl3/MeOH (98.5:1.5)), eluant shaken with 2 M aq. HCl, evapd., recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1021/ja00264a010

Reference yield: 67.0%

: 99688-17-2
iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

: 54606-49-4
3-Methylamino-2,2,5,5-tetramethyl-1-pyrrolidinyloxy

: 99688-21-8
iron(III) 5-(2-((((2,2,5,5-tetramethyl-1-oxypyrrolidin-3-yl)methylene)amido)carbonyl)phenyl)-10,15,20-tri-p-tolylporphyrin chloride

Guidance literature:: With hydrogenchloride; oxalyl dichloride; In tetrahydrofuran; benzene; C2O2Cl2 added to soln. of Fe porphyrin in dry C6H6, stirred at room temp. for 2 h, evapd. in vac., dried in vac. for 2 h, dissolved in dry THF, 3-(aminomethyl)-2,2,5,5-tetramethyl-1-oxypyrrolidinyl added, refluxed gently for 3 h; evapd. in vac., chromd. (SiO2, CHCl3/MeOH (98.5:1.5)), washed with 0.1 M HCl, evapd., recrystd. from CHCl3/hexane; elem. anal.;
DOI:10.1021/ja00264a010

Reference yield: 60.0%

: 99688-17-2
iron(III) 5-(2-carboxyphenyl)-10,15,20-tri-p-tolylporphyrin chloride

: 56674-44-3
4-(aminomethyl)-2,2,6,6-tetramethyl-1-oxy-piperidin-4-yl

: 99688-22-9
iron(III) 5-(2-((((2,2,6,6-tetramethyl-1-oxypiperidin-4-yl)methylene)amido)carbonyl)phenyl)-10,15,20-tri-p-tolylporphyrin chloride

Guidance literature:: With hydrogenchloride; oxalyl dichloride; In tetrahydrofuran; benzene; C2O2Cl2 added to soln. of Fe porphyrin in dry C6H6, stirred at room temp. for 2 h, evapd. in vac., dried in vac. for 2 h, dissolved in dry THF, 4-(aminomethyl)-2,2,6,6-tetramethyl-1-oxy-piperidin-4-yl added, refluxed gently for 3 h; evapd. in vac., chromd. (SiO2, CHCl3/MeOH (98.5:1.5)), washed with 0.1 M HCl, evapd., recrystd. from CHCl3/hexane; elem. anal.;
DOI:10.1021/ja00264a010